A countercurrent liquid-liquid extractor

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1954-09-03
Authors
Wilhelm, Harley
Foos, Raymond
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Ames National Laboratory

Ames National Laboratory is a government-owned, contractor-operated national laboratory of the U.S. Department of Energy (DOE), operated by and located on the campus of Iowa State University in Ames, Iowa.

For more than 70 years, the Ames National Laboratory has successfully partnered with Iowa State University, and is unique among the 17 DOE laboratories in that it is physically located on the campus of a major research university. Many of the scientists and administrators at the Laboratory also hold faculty positions at the University and the Laboratory has access to both undergraduate and graduate student talent.

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Abstract

A novel countercurrent liquid-liquid extractor is presented and illustrated with applications. The apparatus consists essentially of an assembly of mixer-settlers, feeders, reservoirs, and flow lines that are made of glass or other chemical resistant materials. In operation this multistage assembly rotates intermittently in one direction on a horizontal axis causing the immiscible phases to progress to opposite ends of the unit. Details for the construction of the extractor and its principles of operation are given. Extractors of this design are applicable to experimental work and to the preparation of pure compounds in quantity.

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