The nano — sized materials are the advanced materials developed in the eighties[1]and being called nanocrystalline materials, ultra — fine grained materials or nanophase materials. Because there are a lot of interfaces within the nano — scaled materials, the volume fraction occupied by the interface is comparable with that of particles. The particle size effect and disordering effect of interface exist in the materials. They are referred to have“gaslike” structure. So the nano — sized materials have a number of advantages excelling to the traditional materials properties. Many new phenomena have been discovered from the investigations of their optical and electric properties. However few works are related to their mechanical and ultrasonic properties.