Limitations of ceramic materials such as brittleness, low tensile strength and low fracture toughness are being overcome with the introduction of ceramic matrix composites. The mechanical behavior of these fiber-reinforced composites strongly depends on the fiber-matrix bonding condition. If the bonding is too weak, there is poor stress transfer. On the other hand, for a case of very strong bond, the material behaves in a brittle fashion. Recently, photomicroscopic observations were made and the macroscopic behavior of the material was related to the failure mechanisms and damage development under loading [1]. However, this method is destructive, limited to damage on the surface only and cannot easily detect fiber-matrix debonding. Since fiber-matrix debonding is an important indicator of material response it is important to investigate it nondestructively. An effort was made to correlate macroscopic response with microscopic observations and real-time ultrasonic measurements in a unidirectional silicon carbide/glass ceramic composite under longitudinal tensile loading [2].